美國康塔儀器公司與OXFORD合作開發(fā)的Optistat® DN低溫恒溫裝置,專用于Autosorb-1系列儀器,從此,Autosorb-1實(shí)現(xiàn)了在77K到200K之間進(jìn)行無限制氣體吸附實(shí)驗(yàn)的可能.
To meet a growing need for temperature-specific measurement capabilities in porous materials characterisation, Quantachrome Instruments and Oxford Instruments have collaborated in developing a new cryostat specially designed to provide the precise temperature control required for advanced gas sorption studies on the Autosorb-1. The new cryostat gives researchers the ability to easily perform gas sorption studies at any temperature between 77 K and 200 K (-320°F and -100°F) using only liquid nitrogen as a cryogen, with a 24-hour hold time to enable round-the-clock experiments.
Because the structure and reactivity of solid materials determines how their surfaces interact with gas molecules, monitoring the gas sorption process can provide valuable information about the characteristics of technologically useful solids. Routine evaluation of important materials properties that control their performance – such as surface area, size and shape of pores, chemically active sites, and many others – is possible by quantifying the gas–solid interactions through isothermal gas sorption measurements.
This advance in gas sorption capability allows scientists to make measurements across a wide range of temperatures, without the usual restriction of having only a limited number of specific temperatures using baths of different cryogenic liquids or melting solids. For example, high resolution micro/mesopore analysis by argon adsorption can be performed at 87 K without expense of liquid argon.
技術(shù)參數(shù)：
- 在77K到200K之間進(jìn)行無限制氣體吸附實(shí)驗(yàn)
- 溫度: +/- 0.03K
- 在樣品區(qū)具有三點(diǎn)校正的溫度傳感器
主要特點(diǎn)：
,- 僅用液氮做冷媒, 專用于Autosorb-1系列全自動物理/化學(xué)吸附分析儀
- 可在77K到200K之間進(jìn)行無限制氣體吸附實(shí)驗(yàn)
- 無需液氬在87K進(jìn)行高分辨微孔/介孔氬吸附分析
- 對不同吸附物質(zhì)在不同溫度下進(jìn)行寬范圍的準(zhǔn)確測量
- 吸附熱的準(zhǔn)確測定
